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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2048148Generated: November 1, 2026

HCID 178478361, compound → HCID 178420046, compound

https://huagongshe.com/reaction/2048148

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178478361HCID 178478361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 178420046HCID 178420046—

Reaction Steps

To a solution of example 26 (0.1 g, 0.18 mM) in 10 mL of methanol is added 40 mg Pd/C(10%). The reaction mixture is stirred at RT under hydrogen atmosphere overnight. The reaction mixture is filtered through celite and concentrated. It is then purified by column chromatography and washed with water to obtain the desired compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08592591B2
Source datasetuspto-grants-2013_11
ORD IDord-91110df4b7754664b67428c6ae3fbb2a
Source noteuspto-grants-2013_11