Ethyl 2-[(2'-cyanobiphenyl-4-yl)methyl]-3-oxohexanoate → HCID 67009893, compound

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Reaction Conditions

Reaction Steps

A mixture of ethyl 2-[(2′-cyanobiphenyl-4-yl)methyl]-3-oxohexanoate (0.89 g) and 5-methyl-N-(6-methyltetrahydro-2H-pyran-3-yl)-4H-1,2,4-triazol-3-amine (0.25 g) was stirred at 250° C. for 20 min under microwave irradiation. The obtained reaction mixture was purified by silica gel column chromatography to give the title compound as a colorless solid (0.18 g, 30%).

Provenance & Evidence