HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 12717836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 1,3,5-Triaza-7-phosphaadamantane | HCID 143061 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 12717836 | HCID 12717836 | 74.2% |
Reaction Steps
Following the procedure outline in Example 6, 3.14 g (0.02 mol) of 1,3,5-triaza-7-phosphaadamantane was hydrolyzed with a solution of 25 g (0.15 mol) of 48% hydrobromic acid and 40 g of water, giving, after workup, 5.4 g (74% yield) of tris(aminomethyl)phosphine trihydrobromide as a white, crystalline solid, dec. 214° C. without melting.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04196149 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-d7e7e3b9762f447f9ba0112269cf99e1 |
| Source note | uspto-grants-1980_04 |