HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-(14-Methylpentadecyl)aminobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Ethyl 4-(14-methylpentadecyl)aminobenzoate | HCID 20437387 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-(14-Methylpentadecyl)aminobenzoic acid | HCID 20437364 | — |
Reaction Steps
A 4 g. (10.3 m mole) sample of ethyl 4-(14-methylpentadecyl)aminobenzoate is hydrolyzed with 2.0 g. (3 eq) 85% potassium hydroxide in 60 ml. 95% ethanol by refluxing the solution for 5 hours. The solution is cooled, diluted with 100 ml. water and acidified to pH 4.5 with 37% hydrochloric acid. The precipitate is collected and dried in vacuo to yield the title compound as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04196208 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-6d87d1a03c884721990e969d5deee5f9 |
| Source note | uspto-grants-1980_04 |