HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Methylthio)benzothiazole → HCID 20344652, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Methylthio)benzothiazole | HCID 11989 | — |
| Reactant | HCID 20344651 | HCID 20344651 | — |
| Product | HCID 20344652 | HCID 20344652 | — |
Reaction Steps
4-Octadecyloxycarbonylbenzyl bromide (4.7 g, Step 2) and 2-methylmercaptobenzothiazole (2.5 g) were heated together for 35 minutes/190°-195° C. The mixture was cooled and triturated with ligroin to produce a solid which was recrystallized from pyridine/methanol to form the product; yield 4.5 g (81%), m.p. 105°-107° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04197080 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-ff51cafac6964eb79412a6d92a0a7765 |
| Source note | uspto-grants-1980_04 |