HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-4-dimethylamino-2-methoxybenzoic acid → N-[1-(4-fluorobenzyl)-3-pyrrolidinyl]-5-chloro-4-dimethylamino-2-methoxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-4-dimethylamino-2-methoxybenzoic acid | HCID 11075202 | — |
| Reactant | 1-[(4-Fluorophenyl)methyl]pyrrolidin-3-amine | HCID 16244573 | — |
| Product | N-[1-(4-fluorobenzyl)-3-pyrrolidinyl]-5-chloro-4-dimethylamino-2-methoxybenzamide | HCID 20344828 | — |
Reaction Steps
Following the procedure set forth in general method A supra using 1.15 g. of 5-chloro-4-dimethylamino-2-methoxybenzoic acid and 1.07 g. of 3-amino-1-(4-fluorobenzyl)-pyrrolidine, 0.9 g. of N-[1-(4-fluorobenzyl)-3-pyrrolidinyl]-5-chloro-4-dimethylamino-2-methoxybenzamide was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04197243 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-9deef9de529b41ef9b0658daa4d48cf4 |
| Source note | uspto-grants-1980_04 |