HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl orthoacetate → 1,1,1-Triethoxybutane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl orthoacetate | HCID 66221 | — |
| Reactant | 2-Thenoylacetonitrile | HCID 141853 | — |
| Reactant | 5-Methyl-beta-oxo-3-thiophenepropionitrile | HCID 20345054 | — |
| Product | 1,1,1-Triethoxybutane | HCID 371779 | — |
Reaction Steps
The general procedure of Example 11 is repeated but replacing the β-oxo-2-thiophenepropionitrile and triethyl orthoacetate employed in that example with equivalent amounts of 5-methyl-β-oxo-3-thiophenepropionitrile and triethyl orthobutyrate whereby there is obtained the title compound in equally good yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04197310 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-f02fa6a482744ddf92cd3ffb5abf0761 |
| Source note | uspto-grants-1980_04 |