HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → HCID 20345174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Cyclopentadiene | HCID 7612 | — |
| Reactant | 3-Formylbut-2-enyl acetate | HCID 84699 | — |
| Product | HCID 20345174 | HCID 20345174 | 62% |
Reaction Steps
66 g (1 mole) of freshly distilled cyclopentadiene, 71 g (0.5 mole) of 3-formyl-crotyl acetate and 1 g of hydroquinone were heated for 10 hours at 160° C. under nitrogen in a 1 liter stirred autoclave. The reaction mixture was then subjected to fractional distillation, given 65 g of the product (yield: 62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04197411 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-05180581df6641d8b9e7f3cfeb10f0fd |
| Source note | uspto-grants-1980_04 |