HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Aminocephalosporanic acid → HCID 70589106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Aminocephalosporanic acid | HCID 441328 | — |
| Reactant | HCID 178513878 | HCID 178513878 | — |
| Product | HCID 70589106 | HCID 70589106 | 69.8% |
Reaction Steps
7-ACA and 5-mercapto-1,3,4-thiadiazol-2-ylacetamide were reacted as described in example 23a to give the title compound in 69.8% yield; δ(CF3CO2H) 3.93 (2H,s, C2 methylene), 4.63 (2H,s, --CH2CO--), 4.82 (2H,bs, --CH2S--), 5.47 (2H,s, β-lactam protons), 7.2-7.8 (2H,m, --CONH2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198406 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-3a2c65dd25b148a4b7dae85dc3ce734f |
| Source note | uspto-grants-1980_04 |