HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → HCID 20343736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 20343785 | HCID 20343785 | — |
| Product | HCID 20343736 | HCID 20343736 | — |
Reaction Steps
A solution of 24.2 g. (0.10 mole) of benzyl N-hydroxymethylsuccinamate and 28.9 g. (0.11 mole) of triphenylphosphine in 500 ml. carbon tetrachloride is stirred at reflux for 12 hours. After filtering and washing the precipitate with benzene, the organic solvents are removed at 15-20 mm. and 30°-40° C. to give benzyl N-chloromethylsuccinamate of sufficient purity for use in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198413 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-7a72b1a1c7cb407cbf5b90ca56a36d01 |
| Source note | uspto-grants-1980_04 |