Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiocyanic acid, chloromethyl ester → 3-Trifluoromethyl-thiobenzoic acid thiocyanomethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiocyanic acid, chloromethyl ester | HCID 76755 | — |
| 반응물 | HCID 178526136 | HCID 178526136 | — |
| 생성물 | 3-Trifluoromethyl-thiobenzoic acid thiocyanomethyl ester | HCID 54445077 | 69% |
반응 단계
23 g (0.1 mol) of the K salt of 3-trifluoromethyl thiobenzoic acid and 14.3 g (0.13 mol) of chloromethyl thiocyanate were reacted and processed as in Example 1 B. 19 g of a yellowish oil having a density of 1.4 (this corresponds to a yield of 69% of the theoretical conversion).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04198428 |
| 출처 데이터셋 | uspto-grants-1980_04 |
| ORD ID | ord-aa3a7781ad23430db1f2ed350d4ff60c |
| 출처 메모 | uspto-grants-1980_04 |