HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethyl bromide → HCID 20344047, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethyl bromide | HCID 7666 | — |
| Reactant | Benzene, (3-bromopropoxy)- | HCID 68522 | — |
| Reactant | HCID 20344062 | HCID 20344062 | — |
| Product | HCID 20344047 | HCID 20344047 | — |
| Product | HCID 20344054 | HCID 20344054 | — |
Reaction Steps
Samples of 10,11-dihydro-11-oxospiro[dibenz(b,f)thiepin-10,4'-piperidine], free base of Example 3, are separately treated with phenoxypropyl bromide and 2-bromoethylbenzene according to the procedure in Example 12 to obtain 10,11-dihydro-11-oxo-1'-(3-phenoxypropyl)spiro[dibenz(b,f)thiepin-10,4'-piperidine] hydrobromide (Example 13) and 10,11-dihydro-1'-phenethyl-11-oxospiro[dibenz(b,f)thiepin-10,4'-piperidine] hydrobromide, (Example 14), respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198420 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-dada0c547cd4409c8cfa20d0049e48e1 |
| Source note | uspto-grants-1980_04 |