HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylstannane → HCID 12878310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylstannane | HCID 5948 | — |
| Reactant | HCID 12878300 | HCID 12878300 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12878310 | HCID 12878310 | 75.6% |
Reaction Steps
The product obtained by reducing 0.489 g of 3-hydroxy-3-methyl-4-bromo-7-(o-benzyloxyphenyl)-5-heptanolide with 1.34 g of tri-n-butyltin hydride in 4 ml of anhydrous tetrahydrofuran according to the method described in Example 2 (a), was purified by a thin layer chromatography affording 0.300 g of the desired compound as an oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198425 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-43f8f2ab340c401c8c70b106e6795548 |
| Source note | uspto-grants-1980_04 |