HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 54430174, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | HCID 57270480 | HCID 57270480 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | HCID 54430174 | HCID 54430174 | 94.4% |
Reaction Steps
Using 900 mg of 6-[p-(p-fluorobenzyloxy)phenyl]-3-hexen-2-one, 660 mg of ethyl bromoacetate and 260 mg of zinc, the reaction and the purification of the product were carried out according to the method described in Example 1 (a) affording 1.10 g of ethyl 3-hydroxy-3-methyl-7-[p-(p-fluorobenzyloxy)phenyl]-4-heptenoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198425 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-3be2d264c3d5424e98611aa8109a32f8 |
| Source note | uspto-grants-1980_04 |