HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Oxobutanal → HCID 20330052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Oxobutanal | HCID 4686860 | — |
| Reactant | HCID 13442977 | HCID 13442977 | — |
| Product | HCID 20330052 | HCID 20330052 | — |
Reaction Steps
Starting from 2-amino-2-(p-methoxyphenyl)acetonitrile and acetylacetaldehyde, the open-chain intermediate product is prepared, boiling at 180° C./0.03 mm hg. Overall yield of the title compound: 44%, m.p. 198°-200° C. (from diethyl ether).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04198502 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-646863de343f4219b7934077822d28e6 |
| Source note | uspto-grants-1980_04 |