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5-Hydroxypipecolic acid → Methyl L-prolinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Hydroxypipecolic acid | HCID 151730 | — |
| 反応物 | 5-Methoxypipecolic acid methyl ester | HCID 57063014 | — |
| 生成物 | Methyl L-prolinate | HCID 853477 | — |
| 生成物 | 5-Methoxyproline | HCID 70588130 | — |
反応手順
By substituting 5-methoxypipecolic acid methyl ester [preparing from 5-hydroxypipecolic acid by the procedure described in J. Chem. Soc. 429 (1945) for 5-methoxyproline] for the L-proline methyl ester in the procedure of Example 18, 2,3-dehydro-1-(3-acetylthio-1-oxopropyl)-5-methoxypipecolic acid is obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04198515 |
| 出典データセット | uspto-grants-1980_04 |
| ORD ID | ord-bc345ec6ab4d4c7291360d648715cb9e |
| 出典メモ | uspto-grants-1980_04 |