Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | HCID 20298687 | HCID 20298687 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20298673 | HCID 20298673 | 92.1% |
Reaction Steps
5-Methoxy-2-[3-(4-morpholinyl)propoxy]-benzaldehyde (33.4 g) and 14.5 g of phenethylamine are refluxed in 120 ml. of toluene for about 1 hour. After cooling to about 50° C., the solvent is removed using a rotary evaporator and the oily residue is distilled to give 42.1 g of the title compound, boiling point 240°-245° C. at 0.2-0.3 mm of Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04199528 |
|---|
| Source dataset | uspto-grants-1980_04 |
|---|
| ORD ID | ord-c0b8a24627ba415c89c13a8a7ad827f1 |
|---|
| Source note | uspto-grants-1980_04 |
|---|
