HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2E,6E)-2-[(3E)-4,8-Dimethylnona-3,7-dien-1-YL]-6-methylocta-2,6-diene-1,8-diol → (E,E,E)-7-hydroxymethyl-3,11,15-trimethyl-2,6,10,14-hexadecatetraen-ol disulfate pyridine salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2E,6E)-2-[(3E)-4,8-Dimethylnona-3,7-dien-1-YL]-6-methylocta-2,6-diene-1,8-diol | HCID 6373042 | — |
| Reactant | Pyridine sulfate | HCID 11789763 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | (E,E,E)-7-hydroxymethyl-3,11,15-trimethyl-2,6,10,14-hexadecatetraen-ol disulfate pyridine salt | HCID 86736496 | — |
Reaction Steps
Following the same manner as in Example 26, the reaction was conducted with 3.0 g of (E,Z,E) and (E,E,E)-7-hydroxymethyl-3,11,15-trimethyl-2,6,10,14-hexadecatetraen-1-ol and 5.0 g of anhydrous sulfuric acid-pyridine reagent in anhydrous benzene and after-treatment was conducted to afford 4.4 g of the end product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04199519 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-c404477cb6fc4a3f96fe1a285ea8ee29 |
| Source note | uspto-grants-1980_04 |