HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → HCID 12477044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | 1,3-Cyclohexadiene | HCID 11605 | — |
| Reactant | HCID 15960476 | HCID 15960476 | — |
| Product | HCID 12477044 | HCID 12477044 | 93% |
Reaction Steps
A 30 ml solution of ethylene dichloride containing 3.3 g (0.025 mole) of 2-methyl-4-isothiazolin-3-one 1-oxide and 2.0 g (0.025 mole) of cyclohexadiene is heated at 52°-53° C. and stirred overnight. The solution is concentrated to give 4.9 g (93%) of a white solid, m.p. 118°-120° C. which can be recrystallized from ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04199591 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-950792d6515a469785398eb4c88e7451 |
| Source note | uspto-grants-1980_04 |