(2-(Methylthio)ethyl)amine → HCID 54297576, compound

HRID 2050043Notes

Reaction equation

HRID 2050043 reaction equation
[CH3:1][C:2]([O:5][C:6]([N:8]([C@H:10]([C:18]([OH:20])=O)[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH3:9])=[O:7])([CH3:4])[CH3:3].[CH3:21][S:22][CH2:23][CH2:24][NH2:25]>>[CH3:21][S:22][CH2:23][CH2:24][NH:25][C:18](=[O:20])[C@H:10]([CH2:11][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1)[N:8]([C:6]([O:5][C:2]([CH3:1])([CH3:3])[CH3:4])=[O:7])[CH3:9]

Participants

3

Reactant 2

HCID 87697(2-(Methylthio)ethyl)amineHCID 7010602Boc-N-Me-Phe-OH

Product 1

HCID 54297576HCID 54297576, compound

Procedure

This was prepared by coupling of BOC Me Phe OH with 2-methylthioethylamine by the method of Example 1(b) The product was obtained as an oil. Rf1G=0.71 Rf32A=0.48

Workup

  1. customwas obtained as an oil

Sources & evidence

ORD record
ord-068461492a924166a806adaf5ef32e38
Source dataset
uspto-grants-1980_04
Patent number
US04199568

Reaction notes

Loading…