HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 12898559, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 12898558 | HCID 12898558 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12898559 | HCID 12898559 | — |
Reaction Steps
Add ethyl 2-[4-(hexafluoro-2-methoxy-2-propyl)-2,6-dimethylphenoxy]acetate (2.6 g=6.7 mmol) to 30 ml 1.0 N NaOH. Add 20 ml methanol and reflux 3 hours. Acidify with 1.0 N HCl and extract with ether. Dry, concentrate and recrystallize the combined extracts from hexane to obtain, as a white solid, 2-[4-(hexafluoro-2-methoxy-2-propyl)-2,6-dimethylphenoxy]acetic acid, m.p. 105°-108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04199597 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-ff2a501427ca40489ca1d92a9be8675e |
| Source note | uspto-grants-1980_04 |