HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 4763834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | p-Fluoronitrobenzene | HCID 9590 | — |
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 4763834 | HCID 4763834 | — |
Reaction Steps
A mixture of 32.4 g (0.3 mol) of m-aminophenol and p-nitrofluorobenzene (0.15 mol) was boiled under reflux for 10 days in 400 ml of water and then poured into dilute hydrochloric acid, followed by extraction with ethyl acetate, washing 2 to 3 times with dilute hydrochloric acid and then concentrated. The deposited crystals were washed with hot benzene, cooled and then filtered. The yield was 26 g and the melting point was 158°-160° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04200466 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-7715058449834658aa8f9d7054813ceb |
| Source note | uspto-grants-1980_04 |