3,4-Dichloroaniline → HCID 20342330, compound

HRID 2050203Notes

Reaction equation

HRID 2050203 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[Cl:9])[NH2:5].[C:10]([C:13]1[CH:20]=[CH:19][C:16]([CH:17]=O)=[CH:15][CH:14]=1)([OH:12])=[O:11]>>[C:10]([C:13]1[CH:20]=[CH:19][C:16]([CH:17]=[N:5][C:4]2[CH:6]=[CH:7][C:8]([Cl:9])=[C:2]([Cl:1])[CH:3]=2)=[CH:15][CH:14]=1)([OH:12])=[O:11]

Participants

3

Reactant 2

HCID 72573,4-DichloroanilineHCID 120884-Formylbenzoic acid

Product 1

HCID 20342330HCID 20342330, compound

Procedure

Equimolar amounts of 3,4-dichloroaniline and p-carboxybenzaldehyde are stirred together at room temperature to give a nearly quantitative yield of N-(p-carboxybenzylidene)-3,4-dichloroaniline that is recrystallized from ethanol.

Sources & evidence

ORD record
ord-7c75bc220099472eab7c94f64746e67f
Source dataset
uspto-grants-1980_04
Patent number
US04200648

Reaction notes

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