HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57284149, compound → HCID 70589256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57284149 | HCID 57284149 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 70589256 | HCID 70589256 | — |
Reaction Steps
A solution of 80 g. (0.305 m.) of 2,3-dichlorobenzylidenaminoacetaldehyde dimethyl acetal in 300 ml. of ethyl acetate was divided into two equal parts. Platinum oxide (300 mg.) was added to each and the mixtures were shaken under 20 psi H2 for about seven hours. Filtration, evaporation, and distillation afforded 2,3-dichlorobenzylaminoacetaldehyde dimethyl acetal, b.p. 100°-125° C. (0.005 mm.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04200754 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-8635ef22908640c185f2953579a93775 |
| Source note | uspto-grants-1980_04 |