Propargylamine → HCID 178457315、化合物

HRID 2050363ノート

反応式

HRID 2050363 の反応式
C[C:2]1[N:3]=CN[C:6]=1[CH2:7]SCCN.C(C=C(OC)OC)#N.[C:20]([CH:22]=[C:23](OC)[NH:24][CH2:25][CH2:26][S:27][CH2:28][C:29]1[NH:33][CH:32]=[N:31][C:30]=1[CH3:34])#[N:21].C(N)C#C>>[C:20]([CH:22]=[C:23]([NH:3][CH2:2][C:6]#[CH:7])[NH:24][CH2:25][CH2:26][S:27][CH2:28][C:29]1[NH:33][CH:32]=[N:31][C:30]=1[CH3:34])#[N:21]

参加物

5

反応物 4

HCID 239041PropargylamineHCID 226227003,3-Dimethoxyprop-2-enenitrileHCID 178433288HCID 178433288、化合物HCID 178495317HCID 178495317、化合物

生成物 1

HCID 178457315HCID 178457315、化合物

実験手順

When 2-[(4-methyl-1H-imidazol-5-yl)methylthio] ethylamine is reacted with 1-cyano-2,2-bis(methoxy)ethylene according to the procedure of Example 6, Step A, and the resultant 1-cyano-2-methoxy-2-{2-[(4-methyl-1H-imidazol-5-yl)methylthio]ethylamino}ethylene is treated with propargylamine by the procedure of Example 6, Step B, the title compound is produced.

出典と根拠

ORDレコード
ord-a32f1c4bc3dd4a21b54fc0cae47eb2fa
出典データセット
uspto-grants-1980_04
特許番号
US04200760

反応ノート

読み込み中…