HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → cis-3-Azido-2-hydroxymethyl-4-oxoazetidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Methyl (2R,3R)-3-azido-4-oxoazetidine-2-carboxylate | HCID 13566680 | — |
| Product | cis-3-Azido-2-hydroxymethyl-4-oxoazetidine | HCID 86734333 | — |
Reaction Steps
Methyl cis-3-azido-4-oxoazetidine-2-carboxylate was reduced with sodium borohydride as described in Preparation 3 and the product was chromatographed on silica gel with ethyl acetate as eluant to give cis-3-azido-2-hydroxymethyl-4-oxoazetidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04200572 |
| Source dataset | uspto-grants-1980_04 |
| ORD ID | ord-15e7d169cddd4bb89cca48e45f836b69 |
| Source note | uspto-grants-1980_04 |