HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2050486Generated: October 30, 2026
Hydrochloric Acid → 2-Chloroprop-2-en-1-yl chloro(oxo)acetate
https://huagongshe.com/reaction/2050486
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2-Chloro-2-propen-1-ol | HCID 80076 | — |
| Product | 2-Chloroprop-2-en-1-yl chloro(oxo)acetate | HCID 14153243 | — |
Reaction Steps
Oxalyl chloride (130 ml, 1.49 mol) was placed in a dry 3-neck flask under N2 and cooled to 0° C. With stirring, 2-chloroallyl alcohol (138 g, 1.49 mol) was added dropwise in a manner which maintained the temperature at 0°-2° C. and controlled the vigorous evolution of HCl, then allowed to warm to room temperature and held 16 hours and distilled to yield title product, 214 g, b.p. 82°-84° C./23 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05013729 |
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| Source dataset | uspto-grants-1991_05 |
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| ORD ID | ord-3268d0492ac243cf8d5f178a4704cd58 |
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| Source note | uspto-grants-1991_05 |
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