HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Benzyl Bromide → HCID 20058376, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Benzyl Bromide | HCID 7498 | — |
| Edukt | Sodium hydride | HCID 24758 | — |
| Edukt | 8-(3-(Trifluoromethyl)phenyl)-3H,6H-1,4,5a,8a-tetraazaacenaphthylene-3,5(4H)-dione | HCID 15044076 | — |
| Lösungsmittel | Dimethylformamide | HCID 6228 | — |
| Produkt | HCID 20058376 | HCID 20058376 | — |
Reaktionsschritte
To a stirred mixture of 4.0 g of 8-(3-(trifluoromethyl)phenyl)-3H,6H-1,4a,8a-tetraazaacenaphthylene3,5(4H)-dione (prepared as described in Example 14) in 40 ml of dry N,N-dimethylformamide, under nitrogen, is added 650 mg of 60 percent sodium hydride (dispersion in mineral oil). The mixture is stirred at room temperature for 2 hours, then 2.5 g of benzyl bromide is added and the mixture is stirred for 40 hours.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05013737 |
| Quelldatensatz | uspto-grants-1991_05 |
| ORD ID | ord-87673d208b61433f92c9ea4f2c86ea72 |
| Quellennotiz | uspto-grants-1991_05 |