HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54349507, compound → HCID 15132297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54349507 | HCID 54349507 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15132297 | HCID 15132297 | — |
Reaction Steps
A mixture of ethyl 3-dodecyl-3-(2-trimethylsilyl-4-furyl)-2-propenoate (Compound 27, 141 mg, 0.35 mmol) and platinum oxide (28 mg) in ethanol (5 ml) was stirred under hydrogen at room temperature for 2 days. After the solvent and the catalyst were removed, the residue was purified by a silica column using 2% ethyl ether/hexane to give the title ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05013850 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-2f944a38ba0141f2871c80ea576039ff |
| Source note | uspto-grants-1991_05 |