HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-aminopropyl(phenyl)phosphinate → 3-Aminopropyl(phenyl)phosphinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-aminopropyl(phenyl)phosphinate | HCID 19090874 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 3-Aminopropyl(phenyl)phosphinic acid | HCID 10104206 | — |
Reaction Steps
A mixture of 6.83 g of ethyl 3-aminopropyl(phenyl)phosphinate and 30 ml of 20 % hydrochloric acid is refluxed with stirring for 4 hours. The clear solution is evaporated to dryness and the residue is recrystallized from methanol/propylenoxide to give 3-aminopropyl(phenyl)phosphinic acid as a white solid, m.p. 298-300° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05013863 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-6c766cf8b9ec4c44b775d0ef7fd42859 |
| Source note | uspto-grants-1991_05 |