HRID2050741

反应详情

EQUATION

反应方程式

HRID 2050741 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A catalyst was prepared by impregnating 5 grams of the dried and calcined precursor from Example I (Pd/Al2O3) with 5 grams of an ammonium heptamolybdate solution to the point of incipient wetness. The resulting product was dried at room temperature for 10 hours and calcined at 400° C. for 2 hours. The product was then impregnated with 5 grams of the cesium carbonate solution used in Example I to the point of incipient wetness and dried at 120° C. for 8 hours. The ammonium heptamolybdate solution was prepared by dissolving 0.188 grams of (NH4)6MO7O24.4H2O in 5 ml. of deionized water.

WORKUP

后处理

  1. customA catalyst was prepared
  2. customdried
  3. customThe resulting product was dried at room temperature for 10 hours
  4. customdried at 120° C. for 8 hours