Diethylamine → HCID 3936377, compound

Participants

Reaction Steps

In 300 ml of toluene were dissolved 175.4 g of diethylamine and 152.5 g of chloromethylstyrene and the solution was heated to 60°-70° C. for 13 hours. As the reaction progressed, diethylamine hydrochloride precipitated. After filtering off the hydrochloride, the filtrate was washed with water, dried the layer containing toluene with sodium sulfate anhydride, concentrated, and after the addition of 1 g of di-tert-butylcatechol, the mixture was distilled under reduced pressure to provide 120.2 g of diethylaminomethylstyrene as a colorless liquid having a boiling point of 60° C./2 mm Hg.

Provenance & Evidence