Benzyl Alcohol → HCID 19833992, compound

HRID 2050799Notes

Reaction equation

HRID 2050799 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH2:18]([OH:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:25][CH2:18][C:19]3[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=3)[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 244Benzyl AlcoholHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19833992HCID 19833992, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and benzyl alcohol, there is obtained benzyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as an oil, mas spectrum m/e: M+ 328 (4), 237 (44), 194 (100), 179 (21), 165 (30), 91 (62);

Sources & evidence

ORD record
ord-817f12677c7d429f8e0a45555a8b0ce5
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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