13296-56-5 → HCID 19833964, compound

HRID 2050805Notes

Reaction equation

HRID 2050805 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[OH:18][CH2:19][CH2:20][NH:21][C:22](=[O:25])[O:23][CH3:24]>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:18][CH2:19][CH2:20][NH:21][C:22]([O:23][CH3:24])=[O:25])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 1270162113296-56-5HCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19833964HCID 19833964, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and methyl 2-hydroxyethylcarbamate, there is obtained 2-methoxycarbonylamino-ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a resin, mass spectrum m/e: M+ 339 (5), 308 (2), 237 (22), 194 (56), 102 (100);

Sources & evidence

ORD record
ord-7cd5fbd955284c5a9187ae9785070078
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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