HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydropyran-2-methanol → 2-tetrahydro-2H-pyranylmethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydropyran-2-methanol | HCID 7524 | — |
| Reactant | 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile | HCID 19833886 | — |
| Product | 2-tetrahydro-2H-pyranylmethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 70367331 | — |
Reaction Steps
starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and 2-hydroxymethyl-tetrahydropyran, there is obtained 2-tetrahydro-2H-pyranylmethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e: M+ 336 (30), 237 (78), 194 (100), 99 (60);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05015640 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-ad749a1cc1fa4d7e92c4439792e9b9ac |
| Source note | uspto-grants-1991_05 |