1-Phenylethanol → HCID 19834006, compound

HRID 2050809Notes

Reaction equation

HRID 2050809 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH3:18][CH:19]([OH:26])[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:26][CH:19]([CH3:18])[C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 74091-PhenylethanolHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19834006HCID 19834006, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile and α-methylbenzyl alcohol, there is obtained α-methylbenzyl 5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate as a resin, mass spectrum m/e: [M+ 342 (5), 237 (60), 194 (100), 105 (63);

Sources & evidence

ORD record
ord-e4a2f213f6fc41f7a6c4c23a2ca1ffb8
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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