1-Pyrrolidineethanol → HCID 19833949, compound

HRID 2050812Notes

Reaction equation

HRID 2050812 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[OH:18][CH2:19][CH2:20][N:21]1[CH2:25][CH2:24][CH2:23][CH2:22]1>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:18][CH2:19][CH2:20][N:21]3[CH2:25][CH2:24][CH2:23][CH2:22]3)[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 762881-PyrrolidineethanolHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19833949HCID 19833949, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and N-(2-hydroxyethyl)pyrrolidine, there is obtained 2-pyrrolidino-ethyl 5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate as a resin, mass spectrum m/e: M+ 335 (1), 238 (6), 194 (12), 179 (22), 165 (22), 97 (100), 84 (39), 69 (56);

Sources & evidence

ORD record
ord-fd573a30f4c74ad0a990f5293f58db6f
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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