Diethylene Glycol Monomethyl Ether → HCID 19833947, compound

HRID 2050814Notes

Reaction equation

HRID 2050814 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH3:18][O:19][CH2:20][CH2:21][O:22][CH2:23][CH2:24][OH:25]>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:17])[O:25][CH2:24][CH2:23][O:22][CH2:21][CH2:20][O:19][CH3:18])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 8134Diethylene Glycol Monomethyl EtherHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19833947HCID 19833947, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and 2-(2-methoxyethoxy)-ethanol, there is obtained 2-(2-methoxyethoxy)-ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a resin, mass spectrum m/e:M+ 340 (20), 237 (80), 194 (100), 59 (45).

Sources & evidence

ORD record
ord-5240bcc9b318469b95b13b3a7dd249d0
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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