Thiophenol → HCID 19833986, compound

HRID 2050817Notes

Reaction equation

HRID 2050817 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]#[N:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:18]1([SH:24])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16]([S:24][C:18]3[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=3)=[NH:17])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 7969ThiophenolHCID 198338865,7-dihydro-6H-dibenz[c,e]azepine-6carbonitrile

Product 1

HCID 19833986HCID 19833986, compound

Procedure

starting from 5,7-dihydro-6H-dibenz[c,e]azepine-6-carbonitrile and thiophenol, there is obtained phenyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-thiocarboximidate as a syrup, mass spectrum m/e: M+ 330 (3), 220 (70), 179 (100), 165 (85), 110 (74);

Sources & evidence

ORD record
ord-d1d21183fd5e4970b8d51b51b6e3a0f0
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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