化工社化工社 化学情報印刷レポート · 研究参考用
4-(Trifluoromethyl)benzoyl chloride → ethyl N-(p-trifluoromethylbenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(Trifluoromethyl)benzoyl chloride | HCID 67607 | — |
| 反応物 | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate | HCID 19833914 | — |
| 生成物 | ethyl N-(p-trifluoromethylbenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 19834010 | — |
反応手順
In an analogous manner, starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and p-trifluoromethylbenzoyl chloride, there is obtained ethyl N-(p-trifluoromethylbenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 112°-113° C.;
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05015640 |
| 出典データセット | uspto-grants-1991_05 |
| ORD ID | ord-5bb478dfdf7348aead1a989738417ad0 |
| 出典メモ | uspto-grants-1991_05 |