p-Anisoyl chloride → HCID 19833950, compound

HRID 2050824Notes

Reaction equation

HRID 2050824 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:21](Cl)(=[O:30])[C:22]1[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[CH:24][CH:23]=1>>[C:21]([N:20]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH3:19])(=[O:30])[C:22]1[CH:27]=[CH:26][C:25]([O:28][CH3:29])=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 7477p-Anisoyl chlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19833950HCID 19833950, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and p-anisoyl chloride, there is obtained ethyl N-(p-anisoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 71°-78° C.;

Sources & evidence

ORD record
ord-01c98decf5db4cce8326da91082b8556
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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