Benzoyl chloride → HCID 19833931, compound

HRID 2050827Notes

Reaction equation

[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:25])[O:17][CH2:18][CH2:19][O:20][N:21]=[C:22]([CH3:24])[CH3:23])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:26](Cl)(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:26]([N:25]=[C:16]([N:7]1[CH2:8][C:9]2[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=2[C:11]2[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=2[CH2:6]1)[O:17][CH2:18][CH2:19][O:20][N:21]=[C:22]([CH3:23])[CH3:24])(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1

Participants

Reactant 2

HCID 7412Benzoyl chloride

HCID 19833971HCID 19833971, compound

Product 1

HCID 19833931HCID 19833931, compound

Procedure

starting from 2-[(isopropylideneamino)oxy]-ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and benzoyl chloride, there is obtained 2-[(isopropylideneamino)oxy]-ethyl N-benzoyl-5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate as a resin, mass spectrum m/e: M+ 441 (11), 341 (39), 194 (100), 105 (60), 100 (60);

Sources & evidence

ORD record: ord-22f0da13cfc74fcd820245cd8029c45b
Source dataset: uspto-grants-1991_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05015640

Reaction notes

Loading…