Benzoyl chloride → propyl N-benzoyl-5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate

HRID 2050829Notes

Reaction equation

HRID 2050829 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:21])[O:17][CH2:18][CH2:19][CH3:20])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:22](Cl)(=[O:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1>>[C:22]([N:21]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH2:19][CH3:20])(=[O:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1

Participants

3

Reactant 2

HCID 7412Benzoyl chlorideHCID 19833889propyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate

Product 1

HCID 19833907propyl N-benzoyl-5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate

Procedure

starting from propyl 5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate and benzoyl chloride, there is obtained propyl N-benzoyl-5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate as a resin, mass spectrum m/e: M+ 384 (7), 341 (13), 194 (100), 179 (23), 105 (59);

Sources & evidence

ORD record
ord-5aabe2fe6fa8401e98962fd110889d10
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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