3,5-Bis(trifluoromethyl)benzoyl chloride → HCID 54338421, compound

HRID 2050830Notes

Reaction equation

HRID 2050830 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[F:21][C:22]([F:37])([F:36])[C:23]1[CH:24]=[C:25]([CH:29]=[C:30]([C:32]([F:35])([F:34])[F:33])[CH:31]=1)[C:26](Cl)=[O:27]>>[F:21][C:22]([F:36])([F:37])[C:23]1[CH:24]=[C:25]([CH:29]=[C:30]([C:32]([F:35])([F:33])[F:34])[CH:31]=1)[C:26]([N:20]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH3:19])=[O:27]

Participants

3

Reactant 2

HCID 1018563,5-Bis(trifluoromethyl)benzoyl chlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 54338421HCID 54338421, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and 3,5-bis-(trifluoromethyl)benzoyl chloride, there is obtained ethyl N-[3,5-bis-(trifluoromethyl)-benzoyl]-5,7-dihydro-6H-dibenz[c,e]azepine-6 -carboximidate, m.p. 129°-130° C.;

Sources & evidence

ORD record
ord-3597f08cd4064650b6d0b55fe2b27aa7
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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