4-Phenylbenzoyl chloride → HCID 19834000, compound

HRID 2050835Notes

Reaction equation

HRID 2050835 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:21]1([C:30]2[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=2)[CH:26]=[CH:25][C:24]([C:27](Cl)=[O:28])=[CH:23][CH:22]=1>>[C:21]1([C:30]2[CH:31]=[CH:32][CH:33]=[CH:34][CH:35]=2)[CH:22]=[CH:23][C:24]([C:27]([N:20]=[C:16]([N:7]2[CH2:6][C:5]3[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=3[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8]2)[O:17][CH2:18][CH3:19])=[O:28])=[CH:25][CH:26]=1

Participants

3

Reactant 2

HCID 841514-Phenylbenzoyl chlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19834000HCID 19834000, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and biphenyl-4-carboxylic acid chloride, there is obtained ethyl N-(4-biphenylylcarbonyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 52°-58° C.;

Sources & evidence

ORD record
ord-cc355b0c8a584c0c8cad9abb05cab713
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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