化工社化工社 化学情報印刷レポート · 研究参考用
2,6-Dichloro-isonicotinoyl chloride → ethyl N-(2,6-dichloroisonicotinoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dichloro-isonicotinoyl chloride | HCID 2781643 | — |
| 反応物 | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate | HCID 19833914 | — |
| 生成物 | ethyl N-(2,6-dichloroisonicotinoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 19833902 | — |
反応手順
starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and 2,6-dichloropyridine-4-carboxylic acid chloride, there is obtained ethyl N-(2,6-dichloroisonicotinoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 151°-152° C.;
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05015640 |
| 出典データセット | uspto-grants-1991_05 |
| ORD ID | ord-de61f138763343078da55930626d73f1 |
| 出典メモ | uspto-grants-1991_05 |