Acryloyl chloride → HCID 19833946, compound

HRID 2050843Notes

Reaction equation

HRID 2050843 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:21](Cl)(=[O:24])[CH:22]=[CH2:23]>>[C:21]([N:20]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH3:19])(=[O:24])[CH:22]=[CH2:23]

Participants

3

Reactant 2

HCID 13140Acryloyl chlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19833946HCID 19833946, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and acryloyl chloride, there is obtained ethyl N-(acryloyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e: M+ 320 (11), 291 (19), 194 (100), 55 (15);

Sources & evidence

ORD record
ord-eed6777909a84d3a9805b27848a086fe
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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