HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Difluorobenzoyl chloride → ethyl N-(2,5-difluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Difluorobenzoyl chloride | HCID 588082 | — |
| Reactant | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate | HCID 19833914 | — |
| Product | ethyl N-(2,5-difluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 19833924 | — |
Reaction Steps
starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and 2,5-difluorobenzoyl chloride, there is obtained ethyl N-(2,5-difluorobenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e: M+ 406 (4), 377 (18), 194 (100), 141 (49);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05015640 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-8b8e07c953af4d5db9be84a7b1974d28 |
| Source note | uspto-grants-1991_05 |