4-(Trifluoromethoxy)benzoyl Chloride → HCID 19833978, compound

HRID 2050861Notes

Reaction equation

HRID 2050861 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[F:21][C:22]([F:34])([F:33])[O:23][C:24]1[CH:32]=[CH:31][C:27]([C:28](Cl)=[O:29])=[CH:26][CH:25]=1>>[F:21][C:22]([F:33])([F:34])[O:23][C:24]1[CH:32]=[CH:31][C:27]([C:28]([N:20]=[C:16]([N:7]2[CH2:6][C:5]3[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=3[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8]2)[O:17][CH2:18][CH3:19])=[O:29])=[CH:26][CH:25]=1

Participants

3

Reactant 2

HCID 1421104-(Trifluoromethoxy)benzoyl ChlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19833978HCID 19833978, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and p-(trifluoromethoxy)-benzoyl chloride, there is obtained ethyl N-[p-(trifluoromethoxy)-benzoyl]-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e: M+ 454 (1), 425 (11), 194 (100), 189 (40);

Sources & evidence

ORD record
ord-316560358712472788eb539d5fdd0cd8
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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