2-Methylbenzoyl chloride → HCID 19833952, compound

HRID 2050862Notes

Reaction equation

HRID 2050862 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:21]1([CH3:30])[C:22]([C:27](Cl)=[O:28])=[CH:23][CH:24]=[CH:25][CH:26]=1>>[C:21]1([CH3:30])[C:22]([C:27]([N:20]=[C:16]([N:7]2[CH2:6][C:5]3[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=3[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8]2)[O:17][CH2:18][CH3:19])=[O:28])=[CH:23][CH:24]=[CH:25][CH:26]=1

Participants

3

Reactant 2

HCID 702762-Methylbenzoyl chlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19833952HCID 19833952, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and o-toluoyl chloride, there is obtained ethyl N-(o-toluoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum: m/e: M+ 384 (5), 355 (10), 194 (100), 119 (31);

Sources & evidence

ORD record
ord-af8e08c2517a43868847fc293740c4d9
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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